In this paper, the influences of specimen size and test temperature on the viscoelastic properties of SU-8 photoresist films are described. Films with the thicknesses of 1 μm and 10 μm are subjected to quasi-static uniaxial tensile tests and stress relaxation tests at temperatures ranging from 293 K to 473 K. The average glassy modulus at 293 K is 3.2 GPa, which decreases with an increase in the test temperature irrespective of specimen size. The mean fracture strain depends on film thickness as well as temperature. The fracture strain of the 1-μm thick films is approximately half of that of the 10-μm thick films at each temperature. Stress relaxation tests are conducted for constructing the master curves of the relaxation moduli. There is no apparent thickness dependence on the master curve. Above glass transition temperature, Tg, apparent activation energies for the two films are almost identical, whereas the activation energy for the thinner films is smaller than that for the thicker films below Tg. This size effect is discussed using Fourier transform infrared spectroscopy (FTIR).
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April 2016
Research-Article
Influences of Specimen Size and Temperature on Viscoelastic Tensile Properties of SU-8 Photoresist Films
Takahiro Namazu,
Takahiro Namazu
Associate Professor
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
e-mail: namazu@eng.u-hyogo.ac.jp
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
e-mail: namazu@eng.u-hyogo.ac.jp
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Kenichi Takio,
Kenichi Takio
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
Search for other works by this author on:
Shozo Inoue
Shozo Inoue
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
Search for other works by this author on:
Takahiro Namazu
Associate Professor
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
e-mail: namazu@eng.u-hyogo.ac.jp
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
e-mail: namazu@eng.u-hyogo.ac.jp
Kenichi Takio
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
Shozo Inoue
Department of Mechanical Engineering,
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
University of Hyogo,
2167 Shosha,
Himeji, Hyogo 671-2201, Japan
Contributed by the Materials Division of ASME for publication in the JOURNAL OF ENGINEERING MATERIALS AND TECHNOLOGY. Manuscript received June 5, 2015; final manuscript received December 14, 2015; published online January 21, 2016. Assoc. Editor: Hareesh Tippur.
J. Eng. Mater. Technol. Apr 2016, 138(2): 021002 (5 pages)
Published Online: January 21, 2016
Article history
Received:
June 5, 2015
Revised:
December 14, 2015
Citation
Namazu, T., Takio, K., and Inoue, S. (January 21, 2016). "Influences of Specimen Size and Temperature on Viscoelastic Tensile Properties of SU-8 Photoresist Films." ASME. J. Eng. Mater. Technol. April 2016; 138(2): 021002. https://doi.org/10.1115/1.4032320
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